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    2019-5-25  d) compound 1A obtained by liquid-assisted grinding, e) compound 1A obtained by aging experiment in the presence of acetone vapour and f) simulated pattern for compound 1A . Figure S2. PXRD patterns for experiments involving tpp and 2: a) pure 2 reactant, b) pure tpp reactant, c) compound 2A obtained by solution-based method (from acetone),

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    2019-5-26  Entry variation from “standard condition” Conv. of 1a (%) Yield of 3a (%) b 1 none 96 85 2 600 rpm, 1 x 60 min 76 64 3 800 rpm, 6 x (10 min + 1 min break) 83 73 4 400 rpm, 6 x (10 min + 1 min break) 71 55 5 15 stainless steel grinding balls (5 mm diameter) 46 24 a Reaction condition : 1a (0.3 mmol), 2a (165.8 mg, 1.8 mmol), Pd(OAc)

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    The Suzuki–Miyaura cross-coupling reaction is one of the most reliable methods for the construction of carbon–carbon bonds in solution. However, examples for the corresponding solid-state cross-coupling reactions remain scarce. Herein, we report the first broadly applicable mechanochemical protocol for a sol

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  • Solid-state Suzuki–Miyaura cross-coupling reactions ...

    The Suzuki–Miyaura cross-coupling reaction is one of the most reliable methods for the construction of carbon–carbon bonds in solution. However, examples for the corresponding solid-state cross-coupling reactions remain scarce. Herein, we report the first broadly applicable mechanochemical protocol for a sol

  • 2015 high school football preview The Washington

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  • Hall, United Way Invitational celebrate 25 years of

    2019-3-20  Hickory businessman John Hall started the United Way Invitational 25 years ago, growing it into one of the premier cross-country events of the season. Aaron Schnautz/Record Facebook

  • The American Society of Mechanical Engineers - ASME

    ASME (American Society of Mechanical Engineers) promotes the art, science practice of multidisciplinary engineering around the globe.

  • IHS Markit Standards Store Engineering Technical ...

    IHS Markit will be hosting two events with multiple ASME Learning Development course. The courses provide premier training on critical ASME Codes and Standards. Code courses are developed and presented by respected industry experts who understand and can communicate code and standard relevance and their impact on safety, quality and integrity.

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